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HRID85016

反应详情

EQUATION

反应方程式

HRID 85016 的结构方程式

REACTANTS

反应物

5
结构：OB(O)c1ccc2[nH]ccc2c1
HCID2734361

Indole-5-boronic acid

C8H8BNO2

结构：COc1cc(B(O)O)cc(OC)c1OC
HCID2734390

3,4,5-Trimethoxyphenylboronic acid

C9H13BO5

结构：CN(C)c1ccc(B(O)O)cn1
HCID2763271

6-(Dimethylamino)pyridine-3-boronic acid

C7H11BN2O2

结构：Cc1ccc(S(=O)(=O)n2cc(I)c3cc(Br)cnc32)cc1
HCID49759066

5-Bromo-3-iodo-1-(4-methylbenzene-1-sulfonyl)-1H-pyrrolo[2,3-b]pyridine

C14H10BrIN2O2S

结构：Cc1ccc(S(=O)(=O)n2cc(-c3ccc4[nH]ccc4c3)c3cc(Br)cnc32)cc1
HCID66779176

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1ccc(-c2cnc3[nH]cc(-c4ccc(N(C)C)nc4)c3c2)cn1
HCID66778750

未命名化合物

PROCEDURE

实验过程

Compound X was prepared by a method analogous to that described in Example 1 by substituting 6-(dimethylamino)pyridin-3-ylboronic acid for 1H-indol-5-ylboronic acid in the reaction with Intermediate A and 6-(dimethylamino)pyridin-3-ylboronic acid for 3,4,5-trimethoxyphenylboronic acid in the reaction with Intermediate B. HPLC retention time: 1.17 minutes. MS ESI (m/z): 359.4 (M+H)+, calc. 358.