HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 2,6-Di(propan-2-yl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2,6-diisopropylbenzoic acid | HCID 11958990 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Product | 2,6-Di(propan-2-yl)benzoyl chloride | HCID 13068585 | — |
Reaction Steps
A mixture of 2,6-diisopropylbenzoic acid (12.8 g, 0.062 mol), oxalyl chloride (25 mL), and dimethylformamide (2 drops) was stirred overnight at room temperature. The volatiles were removed on the rotary evaporator and the residue dried to yield an orange oil, 12.65 g, 90.9%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06017905 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-44d2c2261a20479093ddf08237117330 |
| Source note | uspto-grants-2000_01 |