Cyclohexanecarboxaldehyde → HCID 53660818, compound

HRID 850336Notes

Reaction equation

[CH2:1]([O:3][C:4](=[O:29])[CH:5]([C:14]1[CH:19]=[C:18]([C:20]([CH3:23])([CH3:22])[CH3:21])[C:17]([OH:24])=[C:16]([C:25]([CH3:28])([CH3:27])[CH3:26])[CH:15]=1)[NH:6][CH2:7][C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)[CH3:2].[CH2:30]1[CH2:35][CH2:34][CH:33]([CH:36]=O)[CH2:32][CH2:31]1>>[CH2:1]([O:3][C:4](=[O:29])[CH:5]([N:6]([CH2:36][CH:33]1[CH2:34][CH2:35][CH2:30][CH2:31][CH2:32]1)[CH2:7][C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)[C:14]1[CH:15]=[C:16]([C:25]([CH3:28])([CH3:27])[CH3:26])[C:17]([OH:24])=[C:18]([C:20]([CH3:22])([CH3:21])[CH3:23])[CH:19]=1)[CH3:2]

Participants

Reactant 2

HCID 16275Cyclohexanecarboxaldehyde

HCID 9930765HCID 9930765, compound

Product 1

HCID 53660818HCID 53660818, compound

Procedure

Synthesized as in Example 2 from Example 2 (0.418 g, 1.05 mmol) and cyclohexyl carboxaldehyde (384 μL, 3.10 mmol). This gave 0.120 g (24%) of product.

Sources & evidence

ORD record: ord-8e72557ee22a45e893450e6800683aea
Source dataset: uspto-grants-2000_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06017918

Reaction notes

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