HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(3-(Benzyloxy)phenyl)ethanamine → m-Tyramine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(3-(Benzyloxy)phenyl)ethanamine | HCID 207415 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | HCID 178418390 | HCID 178418390 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | m-Tyramine | HCID 11492 | 95,5% |
Reaktionsschritte
10% Palladium-carbon catalyst (water content 50%, 86 mg) was added to a solution of 2-(3-benzyloxyphenyl)ethylamine (434 mg, 1.91 mmol, 1.0 eq) in THF (10 ml), and the mixture was stirred at room temperature for 3 hours in a stream of hydrogen. The reaction ma ire was filtered through Celite, and the filtrate was concentrated under reduced pressure to give 2-(3-hydroxyphenyl)ethylamine (250 mg, 95.5%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06017919 |
| Quelldatensatz | uspto-grants-2000_01 |
| ORD ID | ord-a43b55be186346cb9f598980f7df62eb |
| Quellennotiz | uspto-grants-2000_01 |