HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Dimethylethylenediamine → Imidazolidine, 1,3-dimethyl-2-(p-methoxyphenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Dimethylethylenediamine | HCID 8070 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Imidazolidine, 1,3-dimethyl-2-(p-methoxyphenyl)- | HCID 31713 | — |
Reaction Steps
Benzene (20 ml) and N,N'-dimethylethylenediamine (1.56 ml, 14.7 mmol) were added to 4-methoxybenzaldehyde (2 g, 14.7 mmol), and the m tture was refluxed under heating for 5 hours while removing the generated water. Benzene was evaporated to give a crude product of 2-(4-methoxyphenyl)-1,3-dimethylimidazolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06017919 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-f04e82caf67a47b8b98c76be696ccc3f |
| Source note | uspto-grants-2000_01 |