HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19363652, compound → HCID 19363650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19363652 | HCID 19363652 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19363650 | HCID 19363650 | — |
Reaction Steps
A solution of 24-4 (181 mg, 0.38 mmol) in acetic acid (5 mL) was treated with PtO2 (100 mg) and stirred under a hydrogen atmosphere for 1 h. The catalyst was removed by filtration through celite and the residue chromatographed (75% 20:1:1 EtOH/NH4OH/H2O-25% EtOAc) to afford 24-5 as a colorless glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06017926 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-420f6baec5ed40ecb76f4306175c6263 |
| Source note | uspto-grants-2000_01 |