huagongshe.com
HRID851190

反应详情

EQUATION

反应方程式

HRID 851190 的结构方程式

REACTANTS

反应物

2
结构：COc1cccc(O)c1
HCID9007

3-Methoxyphenol

C7H8O2

结构：COC(=O)C1CNCCC1=O.Cl
HCID2724028

Methyl 4-oxopiperidine-3-carboxylate--hydrogen chloride (1/1)

C7H12ClNO3

PRODUCTS

生成物

1
结构：COc1ccc2c3c(c(=O)oc2c1)CNCC3
HCID13136918

未命名化合物

收率 35.8%

PROCEDURE

实验过程

Prepared by the method described for Example 1 from 3-methoxyphenol (16 g, 0.126 moles) and methyl 4-oxo-3-piperidinecarboxylate hydrochloride (25 g, 0.129 moles). Recrystallization from ethanol gave the product (10.43 g), mp 179°-183° C.

WORKUP

后处理

  1. customPrepared by the method
  2. customRecrystallization from ethanol