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HRID851192

反应详情

EQUATION

反应方程式

HRID 851192 的结构方程式

REACTANTS

反应物

2
结构：Oc1cccc(-c2ccccc2)c1
HCID11381

3-Phenylphenol

C12H10O

结构：COC(=O)C1CNCCC1=O.Cl
HCID2724028

Methyl 4-oxopiperidine-3-carboxylate--hydrogen chloride (1/1)

C7H12ClNO3

PRODUCTS

生成物

1
结构：O=c1oc2cc(-c3ccccc3)ccc2c2c1CNCC2
HCID13136920

8-Phenyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[3,4-c]pyridin-5-one

C18H15NO2

收率 54.1%

PROCEDURE

实验过程

Prepared by the method described for Example 1 from 3-phenylphenol (17 g, 0.1 moles) and methyl 4-oxo-3-piperidinecarboxylate hydrochloride (19.3 g, 0.1 moles). The crude material is washed with water and dried to give the product (15 g), mp 250°-270° C.

WORKUP

后处理

  1. customPrepared by the method
  2. washThe crude material is washed with water
  3. customdried