HuagongsheHuagongshe Chemistry Print Report · For research reference only
Resorcinol → 1,2,3,4-Tetrahydro-8-hydroxy-3-(phenylmethyl)5H-[1]benzopyrano[3,4-c]pyridin-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Resorcinol | HCID 5054 | — |
| Reactant | Ethyl 1-benzyl-4-oxopiperidine-3-carboxylate hydrochloride | HCID 102623 | — |
| Product | 1,2,3,4-Tetrahydro-8-hydroxy-3-(phenylmethyl)5H-[1]benzopyrano[3,4-c]pyridin-5-one | HCID 13381781 | — |
Reaction Steps
Prepared by the method described for Example 1 from resorcinol (22 g, 0.2 moles) and 1-benzyl-3-carbethoxy-4-piperidone hydrochloride (59.6 g, 0.2 moles). The product (55 g) is converted to 1,2,3,4-tetrahydro-3-(phenylmethyl)-8-[(1-phenyl-1H-tetrazol-5-yl)oxy]-5H-[1]benzopyrano [3,4-c]pyridin-5-one without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04382939 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-7fbe1d0a18d74ccd9b590f0577de2ff7 |
| Source note | uspto-grants-1983_05 |