HCID 12428590, compound → HCID 178433187, compound

HRID 851273Notes

Reaction equation

HRID 851273 reaction equation
[CH3:1][C:2]1([N:6]=[C:7]=[N:8][C:9]2[CH:10]=[N:11][CH:12]=[CH:13][CH:14]=2)[CH2:5][CH2:4][CH2:3]1.C([N:19]=[C:20]=[N:21]C1C=NC=CC=1)(C)(C)C>>[C:20]([N:21]=[C:7]([NH:8][C:9]1[CH:10]=[N:11][CH:12]=[CH:13][CH:14]=1)[NH:6][C:2]1([CH3:1])[CH2:3][CH2:4][CH2:5]1)#[N:19]

Participants

3

Reactant 2

HCID 12428590HCID 12428590, compoundHCID 20501887HCID 20501887, compound

Product 1

HCID 178433187HCID 178433187, compound

Procedure

By following the procedure of Example 1, but substituting N-1-methylcyclobutyl-N'-3-pyridylcarbodiimide for the N-tert-butyl-N'-3-pyridylcarbodiimide, the desired compound was obtained with a melting point of 210.5°-211.5° C.

Sources & evidence

ORD record
ord-11e6e96115cc41fdaede15aaa5441dbb
Source dataset
uspto-grants-1983_05
Patent number
USRE031244

Reaction notes

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