HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 13125066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Dicyclohexyl ketone | HCID 8403 | — |
| Reactant | HCID 178418630 | HCID 178418630 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13125066 | HCID 13125066 | — |
Reaction Steps
Following the procedures of Example 15, 9.7 g. (0.05 mole) of dicyclohexyl ketone and 14.4 g. (0.1 mole) of cyclopropyl magnesium bromide in dry tetrahydrofuran were reacted and the resulting carbinol dissolved in glacial acetic acid was treated with hydrogen bromide to give 4,4-dicyclohexyl-3-butenyl bromide, b.p. 168°-171° C. (0.1 mm.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04383999 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-35e088ee462e4a7bb2c43e4d4305b931 |
| Source note | uspto-grants-1983_05 |