Methanesulfonamide → HCID 13013731, compound

HRID 851345Notes

Reaction equation

[Cl:1][C:2]1[CH:20]=[C:19]([C:21]([F:24])([F:23])[F:22])[CH:18]=[C:17]([F:25])[C:3]=1[O:4][C:5]1[CH:6]=[CH:7][C:8]([N+:14]([O-:16])=[O:15])=[C:9]([CH:13]=1)[C:10](Cl)=[O:11].[CH3:26][S:27]([NH2:30])(=[O:29])=[O:28]>>[CH3:26][S:27]([NH:30][C:10](=[O:11])[C:9]1[CH:13]=[C:5]([O:4][C:3]2[C:17]([F:25])=[CH:18][C:19]([C:21]([F:24])([F:23])[F:22])=[CH:20][C:2]=2[Cl:1])[CH:6]=[CH:7][C:8]=1[N+:14]([O-:16])=[O:15])(=[O:29])=[O:28]

Participants

Reactant 2

HCID 72879Methanesulfonamide

HCID 20069459HCID 20069459, compound

Product 1

HCID 13013731HCID 13013731, compound

Procedure

Reaction of 5-(2-chloro-6-fluoro-4-trifluoromethylphenoxy)-2-nitro benzoyl chloride with methanesulphonamide to give the required compound, i.e. N-methanesulphonyl-5-(2-chloro-6-fluoro-4-trifluoromethylphenoxy)-2-nitro-benzamide.

Sources & evidence

ORD record: ord-708c54847643499cbfe7f11606b69bad
Source dataset: uspto-grants-1983_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04384135

Reaction notes

Loading…