Dimethylformamide → HCID 131712990, compound

Participants

Reaction Steps

2.06 grams (15 m moles) of 6-AN and 35 ml dry DMF were added to a 250 ml flask and heated under Argon until the 6-AN dissolved. After cooling, but while the mixture was still warm, 25 ml (180 m moles) of Et3N was added to form a cloudy solution which was cooled in dry ice. After 10 minutes, 15 ml of Et3SiCl was added and the mixture kept in the dry ice for an additional 30 minutes. The mixture was left overnight at room temperature.

Provenance & Evidence