3-(Trifluoromethyl)phenylglyoxal → HCID 20501352, compound

Participants

Reaction Steps

The title compound was prepared as in Example 1a from 3-trifluoromethylphenylglyoxal (1.99 g) and 3-(4-carbomethoxyphenyl) propylamine (1.9 g) and crystallised from hexane m.p. 86°-96°. τ(CDCl3) 7.9-8.35 (2H,m), 7.55 (2H, broad, replaceable by D2O), 7.0-7.5 (6H,m), 6.15 (3H,s), 5.3 (1H,m), 2.85 (2H,d,J=8 Hz), 2.3-2.6 (4H,m), 2.05 (2H,d,J=8 Hz).

Provenance & Evidence