Aluminium lithium hydride → HCID 54270255, compound

HRID 851542Notes

Reaction equation

HRID 851542 reaction equation
[CH3:1][C:2](=[CH:6][CH:7]([CH2:11][CH:12]=[CH2:13])[CH2:8][CH:9]=[CH2:10])[C:3](=[O:5])[CH3:4].[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[CH3:1][C:2](=[CH:6][CH:7]([CH2:8][CH:9]=[CH2:10])[CH2:11][CH:12]=[CH2:13])[CH:3]([OH:5])[CH3:4]

Participants

3

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 56609591HCID 56609591, compound

Product 1

HCID 54270255HCID 54270255, compound

Procedure

In an analogous manner to that of Example 7, 17.8 g (0.1 moles) 3-methyl-5-allyl-octa-3,7-dien-2-one (according to Example 6) are reacted with 1.1 g (0.029 moles) LiAlH4.

Sources & evidence

ORD record
ord-26cbe2e77e114a08ab1c36c2e056fa24
Source dataset
uspto-grants-1983_05
Patent number
US04385185

Reaction notes

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