HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 20501536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 88736393 | HCID 88736393 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 20501536 | HCID 20501536 | 87% |
Reaction Steps
This compound was prepared from methyl Z-2-(fur-2-yl)-2-(methoxycarbamoylcyclopent-1-yloxyimino)acetate as described in Preparation 7(d). It was obtained as a pale brown foam, of which part was the sodium salt, νmax (Nujol) 3220 (--NH--), 3700-1800 (bonded OH), 1740, 1707 (--CO2H), 1625, 1512 cm-1 (--CONH--, --CO2θ), τ(DMSO d6) 6.4 (--OCH3), 7.7-8.6 (cyclopentyl), 2.18, 3.20, 3.38 (furyl). Yield 87%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04385177 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-86d9218362594d17b2076f1df4b1d0ad |
| Source note | uspto-grants-1983_05 |