Sodium Hydroxide → HCID 20500782, compound

HRID 851655Notes

Reaction equation

HRID 851655 reaction equation
C[O:2][C:3](=[O:30])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][N:12]([C:22]1[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[CH:24][CH:23]=1)[C:13](=[O:21])[C:14]1[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=1.[OH-].[Na+]>CO>[Cl:20][C:17]1[CH:16]=[CH:15][C:14]([C:13]([N:12]([CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][C:3]([OH:30])=[O:2])[C:22]2[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[CH:24][CH:23]=2)=[O:21])=[CH:19][CH:18]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 54442060HCID 54442060, compound

Product 1

HCID 20500782HCID 20500782, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

As described in example 1(b), the reaction is carried out with 2.8 g (6.5 mmol) of 9-[4-chloro-N-(4-methoxyphenyl)-benzamido]-pelargonic acid methyl ester, 0.3 g (7.8 mmol) of sodium hydroxide and 50 cc. of methanol. Reaction time: 42 hours, reaction temperature: 25° C.

Workup

  1. customReaction time
  2. custom42 hours, reaction temperature
  3. custom25° C.

Sources & evidence

ORD record
ord-053e3a87a0894491890de52916daea28
Source dataset
uspto-grants-1983_05
Patent number
US04386031

Reaction notes

Loading…