HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 73681572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 73681573 | HCID 73681573 | — |
| Reactant | HCID 88732137 | HCID 88732137 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 73681572 | HCID 73681572 | 15.2% |
Reaction Steps
To reaction were subjected 3.7 g of 3-(2-carboxyethyl)-2,6-dimethylbenzothiazolium bromide, 4.3 g of 4-(4-anilino-1,3-butadien-1-yl)-1-ethylquinolinium bromide, 150 ml of ethanol and 5 ml of triethylamine under reflux for one hour. After completion of the reaction, the reaction product was cooled, and the crude crystals thus obtained were purified by means of methanol to obtain 0.9 g of the objective compound (melting point 190° C.) which was glittering green. Its maximum absorption wavelength as measured in triethylamine-containing methanol was 740 nm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04386146 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-2e6e89b4eed247babe28cbfc9b8f0e0f |
| Source note | uspto-grants-1983_05 |