HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 54150769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-[3-(Benzenesulfonyl)propyl]cyclododecan-1-one | HCID 20501203 | — |
| Solvent | Ethylenediamine | HCID 3301 | — |
| Product | HCID 54150769 | HCID 54150769 | 75% |
Reaction Steps
0.720 g (2 mmole) of 2-(3-phenylsulfonyl-prop-1-yl)-cyclododecanone, 0.144 g (6 mmole) of sodium hydride and 10 ml of ethylene-diamine were heated at 100° for 4 hours, then cooled, extracted and finally distilled as indicated hereinabove to afford the desired compound in a 75% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04386220 |
| Source dataset | uspto-grants-1983_05 |
| ORD ID | ord-89eb25617c464f6d83729bd5bd70a19a |
| Source note | uspto-grants-1983_05 |