HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzimidazole → 1-[2-[2-(2-Methoxyethoxy)ethoxy]ethyl]-2-methyl-1H-benzimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzimidazole | HCID 11984 | — |
| Reactant | 1-Chloro-3,6,9-trioxadecane | HCID 547852 | — |
| Product | 1-[2-[2-(2-Methoxyethoxy)ethoxy]ethyl]-2-methyl-1H-benzimidazole | HCID 58927093 | 82% |
Reaction Steps
1-[2-[2-(2-Methoxyethoxy)ethoxy]ethyl]-2-methyl-1H-benzimidazole was synthesized as in Synthesis Example 1 except that an equimolar amount of 2-methylbenzimidazole was used instead of benzimidazole and an equimolar amount of 2-chloroethyl 2-(2-methoxyethoxy)ethyl ether was used instead of 2-chloroethyl methyl ether. Yield 82%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07252925B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-a7fef564d53346fdbb79d60b96c60848 |
| Source note | uspto-grants-2007_08 |