Potassium Carbonate → HCID 22926256, compound

Participants

Reaction Conditions

Reaction Steps

A suspension of 4-cyclohexylphenol (2.5 g), benzyl 2-bromoethyl ether (3.0 g) and potassium carbonate (2.4 g) in N,N-dimethylformamide (50 mL) was stirred at 60° C. for 23 hours. The reaction solution was diluted with water and ethyl acetate. The organic layer was washed with saturated aqueous potassium carbonate solution and saturated ammonium chloride (×2), dried over anhydrous sodium sulfate and concentrated. The residue was purified by silica gel column chromatography to give the title compound as a colorless oil (3.9 g).

Provenance & Evidence