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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 852100Generated: November 1, 2026

Potassium Iodide → HCID 58928263, compound

https://huagongshe.com/reaction/852100

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium IodideHCID 4875—
ReactantPotassium CarbonateHCID 11430—
Reactant2-ChlorobenzylamineHCID 66648—
ReactantHCID 17906346HCID 17906346—
SolventAcetonitrileHCID 6342—
ProductHCID 58928263HCID 58928263—

Reaction Steps

The title compound is prepared from a mixture of 3-[4-(3-bromo-propoxy)-phenyl]-6-fluoro-benzo[d]isoxazole, 2-chlorobenzylamine, potassium carbonate, potassium iodide and 4% aqueous acetonitrile essentially as described above in Example 13. Purity by LC/MS=95%, [M+H]+=411.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07253165B2
Source datasetuspto-grants-2007_08
ORD IDord-ee8a76f2e4864b2f863d53556c3f23c9
Source noteuspto-grants-2007_08