HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 58928305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,4-Difluorobenzylamine | HCID 123572 | — |
| Reactant | HCID 17906346 | HCID 17906346 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 58928305 | HCID 58928305 | — |
Reaction Steps
The title compound is prepared from a mixture of 3-[4-(3-bromo-propoxy)-phenyl]-6-fluoro-benzo[d]isoxazole, 3,4-difluorobenzylamine, potassium carbonate, potassium iodide and 4% aqueous acetonitrile essentially as described above in Example 13. Purity by LC/MS=96%, [M+H]+=413.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253165B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-d6df0e5da7e04733a426bc0f0d613b44 |
| Source note | uspto-grants-2007_08 |