HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 9844301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-Fluorobenzylamine | HCID 67326 | — |
| Reactant | HCID 17906295 | HCID 17906295 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 9844301 | HCID 9844301 | — |
Reaction Steps
The title compound is prepared from a mixture of 2-(4-benzo[b]thiophen-3-yl-phenoxymethyl)-oxirane, 4-fluorobenzylamine and ethanol essentially as described above in Example 94 except that the column chromatography is performed with a graded solvent mixture from 100% ethyl acetate to 10% methanol in ethyl acetate. Purity by LC/MS=100%, [M+H]+=408.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253165B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-5610389f8e1943efb6726dbfa5db0380 |
| Source note | uspto-grants-2007_08 |