N-Methylcyclohexylamine → HCID 61378422, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of N-cyclohexyl-N-methylamine (0.17 g, 0.62 mmol) and 1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione (0.25, 0.56 mmol) in dioxane (7.5 ml) was heated at 100° C. overnight. The solvent was removed under reduced pressure and the crude material was purified by flash chromatography (hexanes ethyl acetate, 1:1) to yield the title compound (0.28 g, 97%) as an orange solid.

Provenance & Evidence