N-Methylcyclohexylamine → HCID 69375594, compound

HRID 852238Notes

Reaction equation

HRID 852238 reaction equation
[CH:1]1([NH:7][CH3:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH2:9]([N:14]1[C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=2[C:17](=[O:24])OC1=O)[CH2:10][CH2:11][CH2:12][CH3:13]>>[CH:1]1([N:7]([CH3:8])[C:17](=[O:24])[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=2[NH:14][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 7514N-MethylcyclohexylamineHCID 143462Benz-3,1-oxazine-2,4-dione, 1-pentyl-

Product 1

HCID 69375594HCID 69375594, compoundYield 67%

Procedure

The title compound (1 g, 67%) was obtained as a yellow solid from N-cyclohexyl-N-methylamine and 1-Pentyl-1H-benzo[d][1,3]oxazine-2,4-dione following the same procedure as described in Preparation 7.

Sources & evidence

ORD record
ord-e93611c064654bfeb20d534bb23d4f0c
Source dataset
uspto-grants-2007_08
Patent number
US07253171B2

Reaction notes

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