N-Methylcyclohexylamine → HCID 69376445, compound

HRID 852239Notes

Reaction equation

HRID 852239 reaction equation
[CH:1]1([NH:7][CH3:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH:9]1([CH2:15][N:16]2[C:21]3[CH:22]=[CH:23][CH:24]=[CH:25][C:20]=3[C:19](=[O:26])OC2=O)[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1>>[CH:1]1([N:7]([CH3:8])[C:19](=[O:26])[C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=2[NH:16][CH2:15][CH:9]2[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 7514N-MethylcyclohexylamineHCID 9856484HCID 9856484, compound

Product 1

HCID 69376445HCID 69376445, compoundYield 67%

Procedure

The title compound (0.3 g, 67%) was obtained as a orange solid from N-cyclohexyl-N-methylamine and 1-Cyclohexylmethyl-1H-benzo[d][1,3]oxazine-2,4-dione following the same procedure as described in Preparation 7.

Sources & evidence

ORD record
ord-c88503a0f5414628b8bdb0ef8cf79ccb
Source dataset
uspto-grants-2007_08
Patent number
US07253171B2

Reaction notes

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