HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → 4-(2-Carboxymethoxyphenoxy)nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | (o-Hydroxyphenoxy)acetic acid | HCID 22783 | — |
| Reactant | Potassium butoxide | HCID 23699084 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | 4-(2-Carboxymethoxyphenoxy)nitrobenzene | HCID 22048504 | — |
Reaction Steps
4-nitro-fluorobenzene and 2-(carboxymethoxy)phenol were reacted together in DMA in the presence of potassium butoxide for 2 hours at 150° C. to yield 4-(2-carboxymethoxy-phenoxy)nitrobenzene, intermediate 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253184B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-b9177533dab244a3b207f7cacafd7748 |
| Source note | uspto-grants-2007_08 |