HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-(4-iodo-1-butyn-1-yl)-4-(trifluoromethyl)- → 2-Methyl-2-{2-methyl-4-[4-(4-trifluoromethyl-phenyl)-but-3-ynylsulfanyl]-phenoxy}-propionic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-(4-iodo-1-butyn-1-yl)-4-(trifluoromethyl)- | HCID 69458210 | — |
| Reactant | 2-(4-Acetylsulfanyl-2-methyl-phenoxy)-2-methyl-propionic acid ethyl ester | HCID 86597820 | — |
| Product | 2-Methyl-2-{2-methyl-4-[4-(4-trifluoromethyl-phenyl)-but-3-ynylsulfanyl]-phenoxy}-propionic acid ethyl ester | HCID 69460333 | — |
Reaction Steps
In analogy to the procedure described in example 1D], 2-(4-acetylsulfanyl-2-methyl-phenoxy)-2-methyl-propionic acid ethyl ester (example 1C]) was reacted with 1-(4-iodo-but-1-ynyl)-4-trifluoromethyl-benzene (example 2E]) to give the title compound as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253192B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-c2813a27cf19480a9a2be4bc121549da |
| Source note | uspto-grants-2007_08 |