HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Acetylsulfanyl-2-methyl-phenoxy)-acetic acid tert-butyl ester → {2-Methyl-4-[5-(4-trifluoromethoxy-phenyl)-pent-4-ynylsulfanyl]-phenoxy}-acetic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Acetylsulfanyl-2-methyl-phenoxy)-acetic acid tert-butyl ester | HCID 11572955 | — |
| Reactant | Methanesulfonic acid 5-(4-trifluoromethoxy-phenyl)-pent-4-ynyl ester | HCID 11616756 | — |
| Product | {2-Methyl-4-[5-(4-trifluoromethoxy-phenyl)-pent-4-ynylsulfanyl]-phenoxy}-acetic acid tert-butyl ester | HCID 11518617 | — |
Reaction Steps
In analogy to the procedure described in example 1D], (4-acetylsulfanyl-2-methyl-phenoxy)-acetic acid tert-butyl ester (example 4A]) was reacted with methanesulfonic acid 5-(4-trifluoromethoxy-phenyl)-pent-4-ynyl ester (example 1G]) to give the title compound a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253192B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-0aee6a9c83e7475b897de2df4e99aeb0 |
| Source note | uspto-grants-2007_08 |