Methanesulfonyl chloride → HCID 86602547, compound

HRID 852422Notes

Reaction equation

[CH3:1][Si:2]([CH3:12])([CH3:11])[C:3]#[C:4][CH2:5][C:6]1([CH2:9][OH:10])[CH2:8][CH2:7]1.[CH3:13][S:14](Cl)(=[O:16])=[O:15]>>[CH3:12][Si:2]([CH3:1])([CH3:11])[C:3]#[C:4][CH2:5][C:6]1([CH2:9][O:10][S:14]([CH3:13])(=[O:16])=[O:15])[CH2:8][CH2:7]1

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 69461118HCID 69461118, compound

Product 1

HCID 86602547HCID 86602547, compound

Procedure

In analogy to the procedure described in example 1G], [1-(3-trimethylsilanyl-prop-2-ynyl)-cyclopropyl]-methanol and methanesulfonyl chloride gave the title compound as yellow oil.

Sources & evidence

ORD record: ord-4d6a43037cbb4f0eae55bdc051d2747d
Source dataset: uspto-grants-2007_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07253192B2

Reaction notes

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