HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 852433Generated: October 30, 2026
Dimethylformamide dimethyl acetal → HCID 72466433, compound
https://huagongshe.com/reaction/852433
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 1-(3-Cyanophenyl)-2-thiourea | HCID 2757972 | — |
| Product | HCID 72466433 | HCID 72466433 | 91% |
Reaction Steps
A mixture of 3 g (16.9 mmol) 1-(3-Cyanophenyl)-2-thiourea and 20 ml N,N-Dimethylformamide dimethyl acetal was heated to 100° C. for 1 h. After evaporation of the volatiles the precipitate was suspended in DCM, filtered and dried to yield 3.56 g (91%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07253197B2 |
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| Source dataset | uspto-grants-2007_08 |
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| ORD ID | ord-8095ad6076e34d819f9678fc783a9013 |
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| Source note | uspto-grants-2007_08 |
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