HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 22499406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 86590841 | HCID 86590841 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 22499406 | HCID 22499406 | — |
Reaction Steps
A mixture of intermediate (27) (0.041 mol) and potassium hydroxide (0.41 mol) in isopropanol (200 ml) was stirred and refluxed for 3 hours and the solvent was evaporated till dryness. Water was added. The mixture was extracted with DCM and the solvent was evaporated, yielding 2-iodo-N-[4-(1-piperazinyl)phenyl]benzamide (intermediate 28).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253157B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-b67a640e59a04c1b8e1a9937979ef31a |
| Source note | uspto-grants-2007_08 |