HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 22499392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 20773936 | HCID 20773936 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 22499392 | HCID 22499392 | 107.3% |
Reaction Steps
A mixture of intermediate (30) (0.0006 mol) and potassium hydroxide (0.006 mol) in isopropanol (5 ml) was stirred at room temperature overnight. The solvent was evaporated. The residue was dissolved in isopropanol/HCl 6N and converted into the hydrochloric acid salt. The precipitate was filtered off and dried, yielding 0.31 g of 4-[4-[[2-(2-furanyl)benzoyl]amino]phenyl]-α-phenyl-1-piperazineacetic acid (intermediate 31).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253157B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-e9b118fdc698432aab6da431ed8b7052 |
| Source note | uspto-grants-2007_08 |