HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyl mercaptan → 1,1-Dimethylethyl {1,1-dimethyl-2-[(2-methylpropyl)thio]ethyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyl mercaptan | HCID 10558 | — |
| Reactant | Methanesulfonic acid 2-tert-butoxycarbonylamino-2-methyl-propyl ester | HCID 11659022 | — |
| Reactant | 1,1-Dimethylethyl [1,1-dimethyl-2-(phenyloxy)ethyl]carbamate | HCID 86602880 | — |
| Product | 1,1-Dimethylethyl {1,1-dimethyl-2-[(2-methylpropyl)thio]ethyl)carbamate | HCID 86602881 | — |
Reaction Steps
1,1-Dimethylethyl {1,1-dimethyl-2-[(2-methylpropyl)thio]ethyl}carbamate (D276) was prepared from 2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2-methylpropyl methanesulfonate (D273) in an analogous manner to 1,1-dimethylethyl [1,1-dimethyl-2-(phenyloxy)ethyl]carbamate (D274) using 2-methyl-1-propanethiol instead of phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253198B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-053338bbbe3c498ebde2bb7254dcc943 |
| Source note | uspto-grants-2007_08 |