Butanoic acid, 2-bromo-, ethyl ester → HCID 178438244, compound
Reaction equation
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH2:3][CH:2]2[NH:8][C:9]([NH2:11])=[S:10].Br[CH:13]([CH2:19][CH3:20])[C:14](OCC)=[O:15]>>[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH2:3][CH:2]2[NH:8][C:9]1[S:10][CH:13]([CH2:19][CH3:20])[C:14](=[O:15])[N:11]=1Participants
3
Procedure
Synthesis was performed from N-bicyclo[2.2.1]hept-2-ylthiourea and ethyl 2-bromobutyrate according to Method C.
Workup
- customSynthesis
Sources & evidence
- ORD record
- ord-1f18b92393c1477aa0beb94581c6b542
- Source dataset
- uspto-grants-2007_08
- Patent number
- US07253196B2
Reaction notes
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