Ethyl 1-bromocyclobutanecarboxylate → HCID 178517990, compound
Reaction equation
[CH:1]1([NH:9][C:10]([NH2:12])=[S:11])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Br[C:14]1([C:18](OCC)=[O:19])[CH2:17][CH2:16][CH2:15]1>>[CH:1]1([NH:9][C:10]2[S:11][C:14]3([C:18](=[O:19])[N:12]=2)[CH2:17][CH2:16][CH2:15]3)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1Participants
3
Procedure
Synthesis was performed from N-cyclooctylthiourea and ethyl 1-bromocyclobutanecarboxylate according to Method D2.
Workup
- customSynthesis
Sources & evidence
- ORD record
- ord-a47a8aed3f2f4e5f9e70458abeb87de4
- Source dataset
- uspto-grants-2007_08
- Patent number
- US07253196B2
Reaction notes
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