Ethyl 1-bromocyclobutanecarboxylate → HCID 178424355, compound

HRID 852698Notes

Reaction equation

HRID 852698 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9]([NH2:11])=[S:10].Br[C:13]1([C:17](OCC)=[O:18])[CH2:16][CH2:15][CH2:14]1>>[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9]1[S:10][C:13]2([C:17](=[O:18])[N:11]=1)[CH2:16][CH2:15][CH2:14]2

Participants

3

Reactant 2

HCID 97595Ethyl 1-bromocyclobutanecarboxylateHCID 2787703N-(2-Methylphenyl)thiourea

Product 1

HCID 178424355HCID 178424355, compound

Procedure

Synthesis was performed from N-(2-methylphenyl)thiourea and ethyl 1-bromocyclobutanecarboxylate according to Method D.

Workup

  1. customSynthesis

Sources & evidence

ORD record
ord-0e3e5544528441f0a9c1a89b3984a6c8
Source dataset
uspto-grants-2007_08
Patent number
US07253196B2

Reaction notes

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