Methyl 1-bromocyclohexanecarboxylate → HCID 178517933, compound
Reaction equation
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH2:3][CH:2]2[NH:8][C:9]([NH2:11])=[S:10].Br[C:13]1([C:19](OC)=[O:20])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1>>[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH2:3][CH:2]2[NH:8][C:9]1[S:10][C:13]2([CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]2)[C:19](=[O:20])[N:11]=1Participants
3
Procedure
Synthesis was performed from N-bicyclo[2.2.1]hept-2-ylthiourea and methyl 1-bromocyclohexanecarboxylate according to Method D.
Workup
- customSynthesis
Sources & evidence
- ORD record
- ord-6f526868f13f49deac7c50adbdb43de5
- Source dataset
- uspto-grants-2007_08
- Patent number
- US07253196B2
Reaction notes
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