HRID852864

反应详情

EQUATION

反应方程式

HRID 852864 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 5-[1-(3-phenyl-allyl)-1H-imidazol-4-yl]-4-(7-phenyl-heptanoylamino)-pent-2-enoic acid ethyl ester (110 mg, 0.21 mmol) and Pd/C (50 mg) in ethanol (100 mL) was subject to hydrogenation (42 psi) for 2 hr. The solution was filtered and the solvent removed. The residue, ESMS 518 (M+H+) was hydrolysed directly without characterisation.

WORKUP

后处理

  1. filtrationThe solution was filtered
  2. customthe solvent removed