Methyl chloroformate → HCID 20658728, compound

HRID 853104Notes

Reaction equation

[Br:1][C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][C:3]=1[F:9].Cl[C:11]([O:13][CH3:14])=[O:12]>>[CH3:14][O:13][C:11](=[O:12])[NH:6][C:5]1[CH:7]=[CH:8][C:2]([Br:1])=[C:3]([F:9])[CH:4]=1

Participants

Reactant 2

HCID 6586Methyl chloroformate

HCID 8218484-Bromo-3-fluoroaniline

Product 1

HCID 20658728HCID 20658728, compound

Procedure

The title compound, m.p. 121–122° C., was prepared in accordance with the general method of example 81a) from 4-bromo-3-fluoroaniline and methyl chloroformate.

Sources & evidence

ORD record: ord-526afba1380049709b8dddb2c43ba0f2
Source dataset: uspto-grants-2007_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07253281B2

Reaction notes

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