Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Perfluorooctanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Hydrofluoric Acid | HCID 14917 | — |
| 반응물 | Octanoyl fluoride, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro- | HCID 67634 | — |
| 생성물 | Perfluorooctanoic acid | HCID 9554 | — |
반응 단계
A 500 ml PFA vessel equipped with a stirrer was used. Water (250 g, 13.9 mol) was temperature conditioned to 15° C. within the vessel, following which C7F15COF (125 g, 0.3 mol) having a purity of 99.9 wt % was added dropwise under stirring. The resulting mixture was a solid-liquid dispersed system composed of an aqueous phase containing the hydrogen fluoride that formed in hydrolysis, and a solid phase of the C7F15COOH that formed in hydrolysis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07253315B2 |
| 출처 데이터셋 | uspto-grants-2007_08 |
| ORD ID | ord-a99c81d4b5ea427c9f587bcc12454bd4 |
| 출처 메모 | uspto-grants-2007_08 |