HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 2-(4-benzyloxy-phenoxy)-N-methyl-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | (4-(Phenylmethoxy)phenoxy)acetic acid | HCID 563696 | — |
| Product | 2-(4-benzyloxy-phenoxy)-N-methyl-acetamide | HCID 11543606 | — |
Reaction Steps
In analogy to the procedure described in Example 1c), the (4-benzyloxy-phenoxy)-acetic acid was reacted with methylamine using 1,1′-carbonyl-diimidazole as the condensation reagent. 2-(4-benzyloxy-phenoxy)-N-methyl-acetamide was obtained as white crystals; MS: m/e=272 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253318B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-e56e0f4e2d8a43afbd9ee36237eb7aa9 |
| Source note | uspto-grants-2007_08 |