HuagongsheHuagongshe Chemistry Print Report · For research reference only
Monobenzone → HCID 69039029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Monobenzone | HCID 7638 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Butanoic acid, 2-bromo-, ethyl ester | HCID 79039 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 69039029 | HCID 69039029 | — |
Reaction Steps
In analogy to the procedure described in Example 1b), the alkylation of 4-benzyloxy-phenol [Example 2a)] with ethyl (RS)-2-bromobutyrate in acetone using cesium carbonate as the base yielded the (RS)-2-(4-benzyloxy-phenoxy)-butyric acid ethyl ester as a brown oil; MS: m/e=314 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07253318B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-70a3ca3fb79f4e9ebc580950b124a6d9 |
| Source note | uspto-grants-2007_08 |