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HRID853907

反应详情

EQUATION

反应方程式

HRID 853907 的结构方程式

REACTANTS

反应物

2
结构：N#CC1(CCl)CCCCC1
HCID2794920

1-(Chloromethyl)Cyclohexanecarbonitrile

C8H12ClN

结构：COC[C@@H]1CCCN1S(=O)(=O)c1ccc2c(c1)C1(OCCCO1)C(=O)N2
HCID58932550

未命名化合物

PRODUCTS

生成物

1
结构：COC[C@@H]1CCCN1S(=O)(=O)c1ccc2c(c1)C(=O)C1=NCC3(CCCCC3)CN12
HCID11611743

未命名化合物

PROCEDURE

实验过程

The title compound was prepared as a yellow foam from 5′-{[(2S)-2-(methoxymethyl)pyrrolidin-1-yl]sulfonyl}spiro[1,3-dioxane-2,3′-indol]-2′(1′H)-one and 1-chloromethyl-cyclohexanecarbonitrile (Syn. Comm. 20(12) 1757, 1990) using a procedure similar to that of steps 3-5 of Example 12. NMR (400 Mz, DMSO-d6): consistent. MS: (ES−) m/z 430 [M−H].