HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → Di(pentafluorophenyl)dichlorosilane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | Bis(pentafluorophenyl)diethoxysilane | HCID 11102434 | — |
| Edukt | Pyridinium hydrochloride | HCID 21584435 | — |
| Produkt | Di(pentafluorophenyl)dichlorosilane | HCID 11112867 | — |
Reaktionsschritte
180.93 g (0.400 mol) di(pentafluorophenyl)diethoxysilane, 146 mL (2.00 mol, 237.9 g) thionylchloride and 4.92 g (0.0426 mol) pyridinium hydrochloride are refluxed and stirred for 16 h. Excess of SOCl2 is evaporated and di(pentafluorophenyl)dichlorosilane isolated by vacuum-distillation.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07256467B2 |
| Quelldatensatz | uspto-grants-2007_08 |
| ORD ID | ord-7f0fc20b329444cf9173f33253c5339c |
| Quellennotiz | uspto-grants-2007_08 |