HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Quinoxaline-2-carbaldehyde → 2-Ethenylquinoxaline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Quinoxaline-2-carbaldehyde | HCID 594088 | — |
| Edukt | 5-Ethenylpyrimidine | HCID 639849 | — |
| Produkt | 2-Ethenylquinoxaline | HCID 21803421 | — |
Reaktionsschritte
Prepared in a similar manner to that described for Intermediate 2, replacing 2-vinylpyrazine with 2-vinylquinoxaline.* The product was purified by SPE using cyclohexane:ethylacetate (2:1 v/v) as eluent to provide the title compound as an oil. *{2-Vinylquinoxaline was synthesized from quinoxaline-2-carboxaldehyde using the procedure described in Intermediate 10 for 5-vinylpyrimidine}.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07259163B2 |
| Quelldatensatz | uspto-grants-2007_08 |
| ORD ID | ord-671bd50379a942d7b35f5a21fc1172a5 |
| Quellennotiz | uspto-grants-2007_08 |