HCID 69244338, compound → HCID 69240454, compound

Participants

Reaction Steps

2.4 g of tert-butyl 4-[cis-3-(tert-butyldiphenylsilanyloxy)cyclohexyl]but-2-enoate are dissolved in 35 ml of methanol, and 200 mg of PD (10% on activated carbon) are added. At room temperature, the mixture is stirred under an atmosphere of hydrogen for 7 hours. The catalyst is filtered off through Celite and the filtrate is concentrated under reduced pressure. This gives 2.3 g of tert-butyl 4-[cis-3-(tert-butyldiphenylsilanyloxy)cyclohexyl]-butanoate as an oil. C30H44O3Si (480.75), MS(ESI): 481 (M+H+).

Provenance & Evidence