HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 855463Generated: October 28, 2026
4-Methoxyphenol → HCID 86602782, compound
https://huagongshe.com/reaction/855463
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) | HCID 466102 | — |
| Reactant | HCID 86602783 | HCID 86602783 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86602782 | HCID 86602782 | — |
Reaction Steps
The crude (R)-4-(4-(6-acryloyloxyhexyloxybenzoyloxy)benzoic acid 2-(tetrahydropyran-2-yloxy)-2-phenyl-ethyl ester (11) was dissolved in 35 ml of ethanol and 0.25 g (1 mmole) of pyridinium 4-toluensulfonate and 40 mg of 4-methoxyphenol were added. The mixture was heated at 55° C. for 15 h. After cooling to 0° C. the product precipitated. 3.2 g of a white solid was obtained (60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07261836B2 |
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| Source dataset | uspto-grants-2007_08 |
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| ORD ID | ord-713291c389754a949b6929471a948cbb |
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| Source note | uspto-grants-2007_08 |
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