HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 855516Generated: October 31, 2026
HCID 68805672, compound → HCID 10472227, compound
https://huagongshe.com/reaction/855516
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 68805672 | HCID 68805672 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 10472227 | HCID 10472227 | — |
Reaction Steps
4-(5-Phenylsulfonyl-2-chlorophenyl)piperazine-1-carboxylic acid tert-butyl ester (D4B) was dissolved in 8 ml of 1,4-dioxane/4 M HCl 1:1. The mixture was heated at 60° C. for 1 h. The solvent was evaporated in vacuo to give the title product as a colourless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07262188B2 |
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| Source dataset | uspto-grants-2007_08 |
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| ORD ID | ord-2cfa5eaa9a7745d6b6eb4f35a3cae8a7 |
|---|
| Source note | uspto-grants-2007_08 |
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